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CLS-News Vol.
2 No.
4 October
15, 2003
www.lightsource.ca University
of Saskatchewan, Canada
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- First electrons in the storage ring!
- MOU signed between CLS and Spain's CELLS
- Scientific Advisory Committee- call for members
- Users Meeting & Associated Workshops- Register Now
- Biomaterials Research Using SR Techniques Workshop
- Synchrotron IR Spectroscopy Workshop: Examples and advice from the
experts
- Application of X-ray Absorption Spectroscopy in (Solid-state) Chemistry
- XAS Data Reduction and Analysis
- Automation of Protein Crystallography Beamlines Workshop
- Users Meeting- Sponsors and Exhibitors listing
- Experimental Facilities Update
- Applied Science at the CLS
- Infrared beamlines
- New staff and postings- Postdoctoral Research Associate
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1. First electrons in the storage ring!
(Contact: les.dallin@lightsource.ca)
For the first time, on September 27th, the electron beam made several complete
circuits of the storage ring and all major systems are working as designed.
Beam position monitors indicated that the beam made over three turns around
the ring.
This Sunday, October 12th, the electrons circulated for 21 turns of the
ring. More turns will require using the superconducting cavity which will
be ready for use this week.
Further refinements to the storage ring will take place over the next several
months. These will aim at keeping the electron beam circulating for several
hours at a time and increasing the beam intensity. This will be followed
by commissioning tests of the photon beamlines.
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2. MOU signed between CLS and Spain's CELLS
(Contact: emil.hallin@lightsource.ca)
On Wednesday, October 1st, in the Spanish island of Menorca, a memorandum
of understanding for scientific and technical cooperation in several areas
of mutual interest was signed by the CLS, the University of Saskatchewan
and the Sincrotrón del Vallès (CELLS). CELLS is the most recently
announced synchrotron project, to be built in Barcelona and scheduled for
operations in 2008.
This partnership is the result of a major effort by CLS and CELLS over the
last few months, which started with a visit to the NRC (Ottawa) by Spain's
State Secretariat for Scientific and Technological Policy, Dr. Pedro Morenés
Eulate, followed by a visit to CLS by the Spanish State Secretariat for Scientific
Policy, Dr. Gonzalo Leon, accompanied by a delegation of scientists and government
representatives. These exchanges culminated with the visit to Barcelona and
Menorca by Dr. Emil Hallin, CLS Experimental Facilities Manager.
The 5-year MOU focuses on several mutually beneficial potential areas, including
exchange of technical specifications and design information; assignment of
scientists or engineers for assistance with development or operation of either
facility, or for research activities to complement the scientific programs
at both facilities; development of joint research and development programs
in technical or scientific applications; collaborations with local suppliers
and industry to provide synchrotron services or construction expertise; educational
opportunities including exchange of scientific expertise and trainees and
applications for mutual access to the beam-lines at the respective Synchrotron
Radiation facilities.
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3. Scientific Advisory Committee- Call for members
(Contact: lori.heikoop@lightsource.ca for
William Thomlinson)
Dear Colleague,
The Canadian Light Source Inc. Board of Directors approved the attached
Terms of Reference for the CLSI Science Advisory Committee (SAC). I am writing
to solicit names of possible scientists whom we might ask to join the SAC.
My plan is to have the first SAC in place by the end of this calendar year
so that we can smoothly transition from the old ROC/FAC committees to the
SAC.
The major thrust is to have a SAC comprised of outstanding scientists with
vision and knowledge of the directions of Canadian and International science,
and the directions that CLS must take to be a truly world class facility.
In addition, the SAC will ensure that our peer review systems, facility utilization,
and future resources are optimized.
I am looking forward to assembling a list of outstanding candidates for
our deliberation. As you think about candidates, please think globally, not
just Canadian. The SAC will have a mix of scientists from Canada and other
countries, and from academia and industry. Ultimately, our choices will be
approved by the Board of Directors. If you would like to comment on any of
the individuals that you propose, please do so. That will be of great benefit
to us.
If possible, we would like to have your suggestions by October 26, 2003.
You can request a copy of the terms of reference by contacting: lori.heikoop@lightsource.ca
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4. Users' Meeting & Associated Workshops - Register Now
(Contact: clsuo@lightsource.ca)
(Early Registration & Poster Deadline October 31, 2003. A $20.00 late fee
penalty will be applied thereafter.)
Registration is now open for the 6th Annual Users' Meeting & Associated
Workshops, November 13-15, 2003 at the University of Saskatchewan. This meeting,
organized by the Users' Advisory Committee of the Canadian Light Source,
will be a great opportunity to learn about the progress of the Canadian Light
Source, present your recent synchrotron work or ideas for future work and
meet fellow users.
The following Workshops will also be held in association with the meeting:
- WinXAS Workshop (November 13th and 14th, all day)
- Synchrotron IR spectroscopy: Examples and advice from the experts (November
14th, All Day)
- Automation of Protein Crystallography Beamlines (November 14th, Morning)
- Biomaterials Research Using Synchrotron Radiation Techniques (November
14th, Afternoon)
You are invited to submit posters about your recent or planned synchrotron
work. The Canadian Institute for Synchrotron Radiation will again offer a
prize for the best synchrotron related poster presented by a graduate student
or post-doctoral fellow. The prize will be $1000 to support travel by the
winner to attend a related conference of their choice in the coming year,
and present their work. Poster submission Deadline is October 31, 2003, please
register here:
http://www.lightsource.ca/uac/meeting2003/poster_submission.php
For more information and to register, please visit the meeting web site:
http://www.lightsource.ca/uac/meeting2003
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5. Biomaterials Research using SR Techniques Workshop
(Contact: alex.moewes@usask.ca)
A workshop entitled Biomaterials Research using Synchrotron Radiation Techniques
Workshop will be held on Friday, Nov. 14th, 2003 from 1 p.m. to 5:30 p.m.
at the University of Saskatchewan. The workshop will discuss key questions
in synchrotron-based studies of biomaterials. It will be organized by Alexander
Moewes and Heinz-Bernhard Kraatz and its purpose is to educate and gather
the Canadian biomaterials research community in synchrotron-based studies.
It will provide the input of experienced synchrotron scientists to: 1. address
the different questions that SR-based techniques can answer, 2. discuss problems
in such different sample systems as gases, liquids and solids, 3. explain
the variety of SR-techniques that are employed to study biomaterials.
The workshop will feature the following six speakers:
- D. Castner (Biochemistry, University of Washington),
- A.P. Hitchcock (Chemistry, McMaster University),
- M. Glover (Biochemistry, University of Alberta),
- P. Kennepohl (Chemistry, University of British Columbia),
- J.S. Lee (Biochemistry, University of Saskatchewan),
- J.-H. Guo (Advanced Light Source, Lawrence Berkeley National Laboratory).
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6. Synchrotron IR spectroscopy workshop: Examples and advice from the
experts
(Contact: kmgough@Ms.UManitoba.CA)
An all-day workshop on synchrotron infrared spectroscopy will be held on
Friday Nov. 14, the day preceding the AUM. The goal is to provide a forum
for learning and discussion among experienced users and novices, to address
to the power and the pitfalls in using synchrotron IR in your research.
I) Special note for the non-expert/novice! IR warm-up. 7:45 AM to 9 AM
Two of the workshop organizers Kathy Gough and Ken Schmidt will host a Coffee
Muffins & IR breakfast in the same room as the all day workshop.
Who should attend this early session? If you are interested in the potential
of mid-IR mapping in your research, but have limited experience with it,
plan to attend this early morning session for an introduction to the theory
and practice of this versatile and powerful technique.
II) Morning regular session: a series of talks by national and international
experts on many aspects of experimentation and application. Speakers include:
- Paul Dumas, IR beamline scientist at LURE, Paris
- Tom Tague, IR microscope applications scientist, Bruker Optics
- Kirk Michaelian (NRCan) & Richard Jackson (Bruker Optics) - photoacoustic
IR
- Robert McKellar (NRC-SIMS) Far IR
III) Afternoon Mid-IR and Far IR sessions:
- Discussion of some major practical issues in data collection and analysis,
with topics introduced by workshop organizers (Kathy Gough, Kirk Michaelian,
and Ken Schmidt).
- Bob McKellar will lead a separate group in a "Planning session: instrumentation
for the far infrared beamline".
IV) Tours and demonstrations of the IR endstations at the ring may take
place later in the afternoon (depending on the commissioning schedule). Tim
May, the CLS IR beamline scientist, will join the organizers in hosting this
informal session.
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7. Application of X-ray Absorption Spectroscopy in (Solid-state) Chemistry
- XAS Data Reduction and Analysis
(Contact: jpercival@nrcan.gc.ca)
After a short introduction into the basics of X-ray absorption spectroscopy
XAS (physics, experimental, and data reduction) the workshop will focus on
the practical aspects of XAS data analysis (one third theory, two thirds
hands-on) using the software package WinXAS. On the first day we will work
together on selected examples illustrating the fundamental data reduction
steps (e.g. calibration, background removal, µ(0) fit, FT) and data
analysis steps (XANES reference fitting, principal component analysis, EXAFS
refinements). On the second day the participants will be working on selected
analysis problems and the results obtained and the procedures chosen will
be discussed. The workshop is intended for XAS user with a basic knowledge
about X-ray absorption spectroscopy and XAS data analysis. This 2-day workshop
will take place on Thursday & Friday, November 13, 14.
For program details please go to: http://www.lightsource.ca/uac/meeting2003/workshop1.php
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8. Automation of Protein Crystallography Beamlines Workshop
(Contact: pawel.grochulski@lightsource.ca)
This workshop will be devoted to automated data collection, reduction and
analysis at protein crystallography beamlines. Presentations will be given
by authors of popular programs such as HKL2000, Blu-Ice and Elves, as well
as by developers of some control systems, including autosamplers, from PX
beamlines at BNL, ALS, ESRF and SSRL. This half-day workshop will take place
on the morning of Friday, November 14th.
For program details please go to: http://www.lightsource.ca/uac/meeting2003/workshop3.php
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9. Users Meeting- Sponsors and Exhibitors
(Contact: sandra.ribeiro@lightsource.ca)
We'd like to thank the following sponsors and exhibitors for their support
of the meeting:
Advanced Design Consulting, Inc.
Alberta Synchrotron Institute
Blake Industries, Inc.
Boehringer Ingleheim
Brush Wellman Inc Electrofusion Products
Gamble Technologies Limited
Gammadata Scienta AB
Johnsen Ultravac Inc
Intelvac
KOHZU Precision Co.,Ltd
MKS Products Group
Newport Canada
Norcal Products, Inc.
Oxford Danfysik
Oxford Instruments
Systems for Research
Struck Innovative Systeme GmbH
UMA Group + Full Spectrum Design Group
Varian Vacuum Technologies
VAT, Inc.
WIENER, Plein & Baus, Ltd.
There is limited space available, so please contact us now regarding different
sponsorship opportunities!
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10. Experimental Facilities Update
(Contact: emil.hallin@lightsource.ca)
With all of the major procurement activities concluded, the focus of the
group has shifted to installation activities. This is a significant milestone
in the beamline delivery schedule and we're delighted to have reached it!
Thanks to UMA for all the work they've done in helping us get here. The next
four to six months will involve coordinating the activities of a large number
of vendors to enable the timely delivery and installation of their products
and the closeout of the respective contracts.
As the vendors provide us with their delivery timetables, installation schedules
are being determined for each of the first phase beamlines. The optical diagnostic
beamline is well on the way to completion. The next highest priority for
CLS resources is being put on the two soft x-ray beamlines which should be
operable by the end of this year (the VLS-PGM and the High Resolution SGM).
The two infrared spectrometers will both be operational before the end of
the year, but design issues (now being solved) related to the first mirror
have pushed delivery of some of the optical components into 2004. The Soft
X-ray Spectromicroscopy beamline components should all be in house by February
2004. Vendor supplied schedules for the protein crystallography and micro-XAFS
beamlines have arrived and are being incorporated into the installation schedules
for these two hard x-ray beamlines.
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11. Applied Science at the CLS
(Contact: jeffrey.cutler@lightsource.ca)
Since the beginning of the CLS project the belief has been that an applied
science program could grow to be an important source of exciting science,
while augmenting the CLSI operating budget and making us a leader in the
global synchrotron community.
Target activities would include academic, government, and industry collaborations
(with or without the intent to publish), and support services for non-traditional
users, including small and medium sized enterprises. With this in mind, CLSI
has taken a very proactive role to develop a strong applied science program,
with a particular emphasis, initially, on environmental geochemistry.
Since May of 2000, we have completed 20 projects for approximately 15 different
clients and helped to facilitate another 5 projects through the DARTS program
at Daresbury Laboratory UK. Two of these reports are published, and three
more are in process. This productivity has lead to a growth in our scientific
team to three and a half dedicated staff scientists, whose mission is to
develop and grow various research programs that will showcase the importance
of synchrotron light-based techniques in various environments. Some projects
are also anticipated to evolve into commercial fee-for-service analysis programs.
We are presently in the process of running another 14 projects, and we have
commitment from three Saskatchewan-based industries to co-fund CLSI research
associate positions.
Future objectives include the pharmaceutical sector and plans to evolve
and diversify into untapped areas, such as ag-biotech and advanced materials.
The applied science program will continue to grow as the beamlines come on-line.
The only way CLSI can reach full potential is to continue to work with partners,
and to consider incentives for beamteam members, and the user community at
large. Please stay tuned for further developments: working together we can
reach objectives as limitless as our imaginations!
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12. Infrared beamlines
(Contact: tim.may@lightsource.ca)
A design review covering the Infrared beamlines was held with Advanced Design
Consulting on Sep 26-5. The UHV, rough vacuum and optics sections of the
beamlines were examined and issues clarified. Detailed design of the chambers
and support equipment continues. A second round of the Mid IR FTIR installation
and training occurred with Tim Rider of Bruker Optics last week. Several
components on the Hyperion microscope were installed: the Attenuated Total
Reflection, Grazing Angle, and 36x objectives. The single bounce ATR and
Photoacoustic accessories were also set up.
The optical table, control rack, and utilities have been installed in the
Mid IR hutch. HVAC equipment is being installed in the next month as well.
The Far IR high resolution spectrometer is shipping from Bruker, Germany,
to CLS on Oct 17; installation is scheduled to occur in November.
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13. New Staff and Postings
(Contact: nancy.fetch@lightsource.ca)
We are looking for two Postdoctoral Research Associates with a background
in geochemistry. Please check the "careers" section of our homepage (http://www.lightsource.ca)
or contact jeffrey.cutler@lightsource.ca
Dr. Pavel Dudin is a Visiting Scholar from the Kurchatov Synchrotron Radiation
Center (KSRC) in Moscow and will be working with Dr. Konstantine Kaznatcheev
on the Soft X-ray Spectromicroscopy project. Pavel will be with us until
the end of May 2004 under the auspices of an MOU signed between CLS/UofS
and KSRC/Moscow State University.
Dr. Ning Chen has officially assumed the appointment of Beamline Scientist
for the Hard X-ray micro-XAFS beamline as of October 1, working with Dr.
De-Tong Jiang. Dr. Chen was the Cogema Postdoctoral Research Fellow at CLS
for the previous two years.
Tracy Walker is our new Outreach Coordinator and will working half-time
as a member of the Business Development team. Tracy brings eight years of
teaching experience to CLS.
Dr. Yongfeng Hu is our newest Beamline Scientist, and will be overseeing
the operation of the Variable Line Spacing Plane Grating Monochromator beamline.
Yongfeng comes to us from the Synchrotron Radiation Center in Madison, Wisconsin.
Dr. Colleen Christensen is our new half-time Industry Liaison Scientist
for Life Sciences. Colleen has been the Project Manager of the BioMedical
Imaging Therapy project for the last two years. She will continue this function
half-time.
Dylan Maxwell is the Science Associate who will be working with Dr. Brian
Yates in the Optics Metrology Lab. Dylan is a recent U of S graduate with
an Engineering Physics and Computer Science background and had worked with
Brian this past summer as a Research Assistant.
Alan Duffy is the Science Associate for the Canadian Macromolecular Crystallography
Facility and holds an M.Sc in Physics from the U of S. Alan will be working
with Dr. Pawel Grochulski and starts on November 1/03.
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Last modified: 2009-10-05 13:10:10