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CLS-News Vol. 1 No. 4 February 6, 2002
www.lightsource.ca University of Saskatchewan, Canada
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- Canadian Nuclear Safety Commission (CNSC) approves CLS Phase II commissioning
- Linac Update
- CLS IT Detailed Design
- U of S Workshop on Synchrotron Applications in the Life Sciences -
March 22-23
- Workshop on Advanced Materials - May 2002- McMaster University
- Notes from the UAC
- Canada Research Chair position; U of S; Environmental Earth Sciences
- Synchrotron Radiation
- Science Highlights
- IR Modification of U10B Infrared Microscope adds external detector
for Far-Infrared Spectromicroscopy
- New Developments in soft X-ray microscopy
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1- Canadian Nuclear Safety Commission (CNSC) approves CLS Phase
II commissioning (Contact: Mohamed.Benmerrouche@lightsource.ca )
The CNSC has given the Canadian Light Source the green light to go to “Phase
II commissioning” which consists of completing the commissioning of
the linac to the booster transfer line, commissioning of the booster ring,
and commissioning of the booster-to-storage-ring transfer line. In the Phase
II hearing, held November 15th in Ottawa, CNSC reviewed the measures CLS
has in place for protecting workers, protecting the environment, security,
quality assurance, emergency preparedness, public information, planning for
eventual decommissioning, and liability. On protecting workers, through measures
like shielding, locked areas, worker training, and radiation monitoring,
the Commission said it’s satisfied adequate steps are being taken.
The CNSC is also satisfied with CLS measures to protect the environment,
to ensure the facility’s security, to ensure quality, to be ready to
handle emergencies, to inform the public about the project, and to prepare
for decommissioning.
For the complete text of the Commission’s decision, please go to: www.nuclearsafety.gc.ca/eng/commission/pdf/cls_e.pdf where
the document can be downloaded in pdf format.
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2- Linac Update (Contact: Les.Dallin@lightsource.ca )
CLS commissioning resumed on January 15, 2002. Within a few days the linac
produced a beam of 240 MeV, which is sufficient energy for injection into
the booster. The booster to storage ring transfer line is nearly completed,
and the beam will be taken to the boosterinjection point in the near future.
The booster should be ready for commissioning in March.
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3- CLS IT Detailed Design (Contact: skeeter.abellsmith@lightsource.ca )
EDS recently completed the top-level architecture for the CLS IT infrastructure. During
the development of the IT architecture, EDS interviewed a subset of the scientific
users to establish the high-level IT requirements.
To view the PDF, please go to http://www.lightsource.ca/files/details.php?id=69 and
select "download" or "view". You may also go to http://www.lightsource.ca/files/
and select "CLS IT", then "IT overview", then "download" or "view".
EDS is proceeding to the next phase and their primary approach to gathering
requirements is through interviews with users (and supporting documentation). Each
of the beamline team leaders recommended one or two members as contacts. You
can request a list of the ITA Oversight Committee, the Beamline IT and EDS
Beamline IT contacts by e-mailing skeeter.abellsmith@lightsource.ca
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4- U of S Workshop on Synchrotron Applications in the Life Sciences -
March 22-23 (Contact: Kathryn.warden@usask.ca )
This two-day workshop for the U of S research community on applications
of synchrotron radiation in the life sciences will be held in Place Riel
Theatre. The agenda includes talks by several leading synchrotron scientists
from the U.S. and Canada. The U of S President’s Office, Ag-West Biotech
Inc., and NRC’s Plant Biotechnology Institute sponsor the event.
An agenda and registration information can be seen on the Canadian Light
Source website at www.lightsource.ca All
faculty and students are welcome to attend.
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5- Workshop on Advanced Materials - May 2002- McMaster University (Contact: bimr@mcmaster.ca )
The Brockhouse Institute for Materials Research at McMaster University is
organizing a workshop on "Frontiers in Characterisation of Soft and
Nanoscale Materials” which will take place on May 15, 16, and 17, of
2002. The workshop will focus on applications of electron microscopy, scanning
probe microscopy and optical methods to characterize soft materials including
polymers and biomaterials and a wide variety of nanoscale materials. Workshop
leaders include Detong Jiang (X-ray absorption) and Adam Hitchcock (X-ray
microscopy). The workshop will feature practical sessions with hands-on experience
in advanced materials characterization instrumentation, including operating
and analysing data from a new X-ray microscopy at the Advanced Light Source.
For more information please go to http://www.science.mcmaster.ca/bimr/workshop.html
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6- Notes from the UAC (Contact: Stephen.Urquhart@usask.ca )
I am pleased to welcome four newly elected members to the Users' Advisory
Committee (UAC): Alan Anderson (StFX), Gerald Audette (UAlberta), Brett Moldovan
(USask/Cameco) and Jeanne Percival (NRCan), as well as the re-election of
Adam Hitchcock (McMaster). Tom Tiedje (UBC), who has been active recently
in the exciting developments in the British Columbia Synchrotron Institute,
will serve as the vice chair for 2002, and take over as chair in 2003.
As an advisory committee representing the interests of CLS users, the UAC
has been active on several issues since the Annual Users' Meeting. We are
working with Ron Cavell of the Canadian Institute of Synchrotron Radiation
in promoting a residence for CLS users at the University of Saskatchewan.
In mid-December, the U of S Board of Governors approved a joint graduate
student / researcher residence that will fill this role. As well, the UAC
has responded in detail to a request from the CLS Board for comments on proposed
changes to the organizational structure of the CLS.
2002 will be a busy year for the UAC and an important year for the CLS as
it moves closer to operation. The Annual User Meeting, organized by the UAC,
will be held on November 16, 2002. If you are a future CLS user, your concerns
are the UAC's concerns. Please contact the chair at stephen.urquhart@usask.ca or any
member (see http://www.cls.usask.ca/uac/membership.php for the
UAC membership list).
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7- Canada Research Chair position; University of Saskatchewan; Environmental
Earth Sciences - Synchrotron Radiation (Contact: Jim.basinger@usask.ca )
An outstanding individual is required to establish research excellence in
the application of synchrotron radiation in the area of environmental earth
sciences at the University of Saskatchewan. He/she will have access to the
Canadian Light Source The University invites applications from outstanding
individuals to be nominated for either a Tier One or Tier Two Canada Research
Chair (www.chairs.gc.ca). The successful candidate will also hold a tenurable
faculty appointment in the Department of Geological Sciences. The Department
has 15 full-time faculty, including two endowed research chairs in geochemistry.
The analytical infrastructure in the Department is one of the finest in North
America, with MC-ICP-MS, laser ablation quadrupole ICP-MS, TIMS, IRMS, electron
microprobe, SEM, XRD, and trace-metal clean room).
For more information on the U of S Canada Research Chairs program please
go to
http://www.usask.ca/vpacademic/programs/crc/crc.shtml
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8- Science Highlights
I- IR Modification of U10B Infrared Microscope adds external
detector for Far-Infrared Spectromicroscopy" (Contact: tim.may@lightsource.ca .)
Tim May CLS, Lisa Miller NSLS, Neb Marinkovic CLS/AEC
The Infrared Beamline U10B at NSLS has a new capability being developed for IR
spectromicroscopy. The Continuum microscope has been modified with the addition
of an external long-wavelength detector. The extended bandwidth allows more extensive
fingerprinting of organic samples, and characterization of inorganic materials.
Canadian IR users now have access to this unique new technique. Tim May designed
the transfer optics and the NSLS shop made the parts, which were installed by Tim
and Lisa and Neb in mid-December. It was a busy week getting all of the parts to
fit into place and not disturb the existing optics! A retractable mirror intercepts
the beam before the standard detectors, and redirects it to a focusing optic above
the microscope, where the new detector sits. The design allows rapid changeover
between the normal and external detectors, and different detector types can be
substituted. The liquid He cooled Cu:Ge detector allows spectroscopy below the
750 cm-1 cut-off of the standard MCT-A detector, down to the 400 cm-1 limit of
the KBr beamsplitter. Longer wavelengths into the Far-IR (wavenumbers < 400
cm-1) can be obtained by changing to a Silicon beamsplitter. The performance and
long-wave limit is being evaluated now. The new configuration is called "DICE" for "Detector
Interface for Continuum Enhancement".
For more information please contact Neb marinkov@bnl.gov or
Tim at tim.may@lightsource.ca. This project
is a collaborative PRT effort between CLSI and NSLS.
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II- New Developments in soft X-ray microscopy (Contact: aph@mcmaster.ca )
Over the past 6 years Adam Hitchcock and Tolek Tyliszczak (McMaster University),
in collaboration with researchers from NCSU, the Advanced Light Source (ALS)
and Dow Chemical, have helped to develop soft X-ray transmission X-ray microscopy
(STXM) at the ALS. STXM is a new synchrotron technique with powerful capabilities
for the chemical analysis at the 50 nm spatial scale of soft matter and wet
samples commonly met in polymer, biological and environmental science. A
new beamline and advanced STXM, fully dedicated to STXM microscopy in the
C 1s, N 1s, O 1s regime (270-600 eV), has been built at the ALS over the
past two years, and is now operational. The new instrument features a laser
interferometer based navigation and scanning system which has made a dramatic
improvement in performance of the microscope. The new STXM at the ALS was
partly funded by NSERC. Dr. Hitchcock has a 22% share of the 75% of
the beamtime allocated for the participating research team. Examples of the
current capabilities of the new instrument can be found at http://www.physics.ncsu.edu/stxm/p-stxm-first-results.pdf
The soft X-ray spectromicroscopy facility under construction at the CLS
will provide STXM and a related technique, X-ray photoelectron emission
microscopy (X-PEEM) (highlighted in CLSNews Vol 101). At CLS
both microscopes will be illuminated by a state-of-the-art, high resolution,
undulator beamline which will allow complete polarization control of the
X-rays. This facility will be operational in 2004.
If you plan to use STXM or X-PEEM at the CLS, it would be very helpful in
planning your research to carry out trial experiments in the next 2 years.
An Elmitec X-PEEM has been purchased through an NSERC major installation
grant. It will operate for the next 2 years at SRC (Madison, WI) then be
relocated to CLS. Please contact Dr. Urquhart (stephen.urquhart@usask.ca) to arrange
for a trial X-PEEM experiment. STXM is available now. If you are interested
in exploring the power of STXM for your micro-analysis problems, consider
collaboration with Adam Hitchcock (aph@mcmaster.ca), or apply directly to the ALS independent investigator
program (http://www.als.lbl.gov/als/quickguide/becomealsuser.html). STXM
provides quantitative chemical mapping with 50 nm spatial resolution. STXM
requires soft X-ray translucent samples, which must be very thin (about 100
nm), similar to those in transmission electron microscopy. Soft X-rays penetrate
thin water layers (up to 10 microns) so it is possible to study fully hydrated
samples contained in an appropriate cell with X-ray transparent silicon nitride
windows.
For further information please consult the following web sites: